Document Type
Thesis
Date of Degree Completion
1968
Degree Name
Master of Science (MS)
Department
Chemistry
Committee Chair
L. Clint Duncan
Second Committee Member
Helmi S. Habib
Third Committee Member
Richard W. Hasbrouck
Abstract
The reaction of C6H5SF3, CSF and C12 was studied under a variety of conditions. The reaction run in the presence of a trace of water yielded C6H5SO2F and C1C6H4SO2F. The reaction run in stainless steel at 170°C yielded an amber solid believed to be a polymer with the empirical formula C6H3.67SF2. Chlorination of a C6H5SF3-CSF mixture in monel at 220°C yielded a yellow liquid tentatively identified as a mixture of the new species C6H5SF4C1, FC6H4SF4C1 and C1C6H4SF4C1.
Recommended Citation
Sauer, Dennis T., "Preparation of Phenylsulphur Chloride Tetrafluoride" (1968). All Master's Theses. 975.
https://digitalcommons.cwu.edu/etd/975
Language
English